M. Andou et A. Sawaoka, SINTERABILITY AND FRACTURE-TOUGHNESS OF B ETA-SI3N4 WHISKER-ADDED SILICON-NITRIDE, Nippon Seramikkusu Kyokai gakujutsu ronbunshi, 102(9), 1994, pp. 890-892
Silicon nitride powders containing 5 mass% Y2O3 and 5 mass% MgAl2O4 as
sintering additives were sintered with beta-Si3N4 whisker of 0-90 mas
s% at 1800-degrees-C for 1-3h at 0.1-1 MPa of N2 atmosphere. The silic
on nitride with 0-15 mass% beta-Si3N4 whisker was densified above 90%
of theoretical density in the above conditions. Rod-like beta-Si3N4 gr
ains grew on seeded-beta-Si3N4 whisker. The fracture toughness of Si3N
4 with 15 mass% beta-Si3N4 whisker was 35% higher than that of monolit
hic Si3N4.