Hw. Gao et Pf. Zhang, DETERMINATION OF ANTIMONY IN WASTE-WATER WITH CHROMAZUROL-S BY BETA-CORRECTION SPECTROPHOTOMETRY, Analyst, 119(9), 1994, pp. 2109-2111
Beta correction absorbance can eliminate completely the interference f
rom the excess of chromogenic reagent to give the real absorbance of t
he complex produced. The reaction of antimony and Chromazurol S was de
veloped in pH 5-6 buffer solution. The determination of trace amounts
of antimony in waste water was studied by beta correction spectrophoto
metry using this reaction. The results showed that Beer's law was obey
ed over the concentration range O-1.0 mg l(-1) of antimony. The detect
ion limit is 0.009 mg l(-1), which is low enough to determine antimony
in environmental waters.