Ds. Stone et Kb. Yoder, DIVISION OF THE HARDNESS OF MOLYBDENUM INTO RATE-DEPENDENT AND RATE-INDEPENDENT COMPONENTS, Journal of materials research, 9(10), 1994, pp. 2524-2533
The hardness, H, and rate sensitivity of the hardness, m = partial der
ivative ln H/partial derivative ln epsilon(eff)\x(p), where epsilon(ef
f) is an effective strain rate and x(p) the plastic depth, are measure
d in molybdenum at room and low temperature (160 and 170 K) using as-r
eceived and annealed specimens. Based on these measurements it is foun
d that H separates into two components: one depending on indentation r
ate and temperature, and the other depending on the starting state of
the material. An activation volume is defined, v() = 9kT/mH, which fa
lls within the range of values derived from other experimental techniq
ues. The values of rn obtained from indentation creep, indentation loa
d relaxation, and indentation rate-change experiments agree closely wi
th each other provided a consistent analysis is used. The results of t
hese experiments suggest that the rate- and temperature-dependence of
the hardness can be used to discriminate between strengthening mechani
sms at low temperature.