Wj. Obrien et al., EVALUATION OF SOME PROPERTIES OF AN OPAQUE PORCELAIN FIRED SIMULTANEOUSLY WITH THE BODY PORCELAIN, The Journal of prosthetic dentistry, 72(4), 1994, pp. 414-419
Recently, a porcelain-fused-to-metal opaque porcelain was introduced t
hat does not require a separate firing before application of the body
porcelain. The objective of this study was to determine the properties
of this new opaque porcelain and its ability to bond to metal. The pr
operties studied included flexural strength, linear firing shrinkage,
coefficient of thermal expansion, powder particle size, and ability to
bond to body porcelain and dental alloys. Sintering of this opaque po
rcelain was complete when fired at 1760 degrees F (960 degrees C) with
a linear firing shrinkage of 13.1% +/- 0.2%. No boundary between the
opaque and body porcelains could be found with a scanning electron mic
roscope after firing at 1760 degrees F (960 degrees C). The mean flexu
ral strengths were 99 +/- 7 and 101 +/- 8 MPa respectively, for this o
paque porcelain and a conventional opaque porcelain, and were not sign
ificantly different as assessed with Student's t-test (p = 0.548). The
coefficient of thermal expansion for this opaque porcelain was 13.3 /- 0.2 X 10(-6)/degrees C. Particle size analysis showed a 63% increas
e in the particles below 5 mu m for this opaque porcelain and bonding
to two alloys was adequate as indicated by its cohesive failure. Simul
taneous firing of this special opaque porcelain and body porcelain pro
duced satisfactory sintering, strength, and bonding to metal.