The mechanical properties of nanocomposite Ag-Al2O3 and Fe-SiO2 granul
ar metal films were investigated by low-load indentation and laser ult
rasonic methods. A discontinuity in the rate of change of hardness as
a function of metal volume fraction was observed near the percolation
threshold for the metal. However, the sign of the rate of change was d
ifferent for the two systems. It is suggested that this discontinuity
was the result of a change in deformation mechanism as the percolation
threshold for the softer phase was crossed. The elastic moduli of the
Ag-Al2O3 films as measured by a laser ultrasonic technique displayed
a rule-of-mixtures-type behavior, in contrast to nanoindentation measu
rements that gave a peak in the apparent compliance. Indentation crack
testing indicated that the toughness increased in the Ag-Al2O3 system
when the metallic phase was introduced into the ceramic, but that the
Fe-SiO2 system displayed unexpected and novel fracture behavior.