A rapid solubilization procedure for maize starch, using low-temperatu
re gelatinization in 3 M CaCl2 in combination with 15-30 min of sonica
tion in an iodine-dimethyl sulfoxide solution at a temperature of 65-7
0-degrees-C makes it possible to estimate amylose content of maize sam
ples in less than 1 hr. Results obtained by this technique are equival
ent to those obtained by conventional thermal dissolution of starch in
iodine-dimethyl sulfoxide, which requires overnight heating to obtain
complete solubilization.