ONE-POT SYNTHESIS OF 1,2-O-ISOPROPYLIDENE-ALPHA-D-XYLOFURANOSE

Citation
J. Moravcova et al., ONE-POT SYNTHESIS OF 1,2-O-ISOPROPYLIDENE-ALPHA-D-XYLOFURANOSE, Carbohydrate research, 263(1), 1994, pp. 61-66
Citations number
25
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
ISSN journal
00086215
Volume
263
Issue
1
Year of publication
1994
Pages
61 - 66
Database
ISI
SICI code
0008-6215(1994)263:1<61:OSO1>2.0.ZU;2-4
Abstract
The title compound 1 was prepared by sulfuric acid-catalyzed acetalati on of D-xylose followed by partial hydrolysis with aqueous sodium carb onate added directly to a crude acetalation mixture. The yield of crys talline 1 (mp 42-43 degrees C) was 80%.