A superparamagnetic nanocomposite of silver and iron oxide was synthes
ized by gas condensation. The procedure involved (1) coevaporation of
Silver and iron, (2) in situ oxidation of iron particles, (3) in situ
compaction, and (4) post-annealing in an inert or an oxidizing atmosph
ere. The magnetization plots against H/T fell on a single curve from r
oom temperature to 160 K, thereby providing evidence of superparamagne
tism. Annealing treatment modifies the effective magnetic moment size
and saturation value of magnetization. The present process is a potent
ial synthesis route for magnetic nanocomposites useful for application
s such as magnetic refrigeration, recording and permanent magnets.