A new adduct of C60 with alpha,alpha'-Azoisobutyronitrile has been syn
thesised and characterized by H-1 NMR, C-13 NMR, FTIR, UV-vis, EI Mass
Spectrum and Cyclic Voltammetry Spectrum. The Langmuir trough study o
f this adduct indicates that the introduction of the hydrophilic group
s can reduce the molecular aggregation at the air-water interface.