Y. Katoh et al., MICROSTRUCTURAL RESPONSE OF TITANIUM-MODIFIED AUSTENITIC STAINLESS-STEELS TO NEUTRON EXPOSURE OF 70-DPA IN FFTF MOTA/, Journal of nuclear materials, 215, 1994, pp. 464-470
JPCA, a titanium-modified austenitic stainless steel, in solution-anne
aled or cold-worked condition and a compositionally modified JPCA in s
olution-annealed condition were examined by transmission electron micr
oscopy following irradiation in FFTF/MOTA to an exposure level of up t
o about 70 dpa at 390 to 600 degrees C. At lower temperatures, ail the
materials developed qualitatively similar cavity-, dislocation- and p
recipitate-microstructures. The lower-temperature swelling peak, which
appeared at near 410 degrees C, was more efficiently suppressed by ph
osphorus addition than cold-working. Irradiation at or above 520 degre
es C produced substantially large swelling in solution-annealed JPCA.
The cavities contributed to this higher-temperature swelling developed
in association with M(6)C-type precipitates. Neither cavities other t
han very small helium bubbles nor massive particles of M(6)C-type prec
ipitates were observed in cold-worked and phosphorus-modified material
s, in which MC-type precipitates developed at very high concentration.
The effect of pre-irradiation microstructure and compositional modifi
cation on the behavior of these precipitates is discussed.