Ca. Black et al., INFLUENCE OF HIGH-DOSE NEUTRON-IRRADIATION AT 385-DEGREES-C AND 750-DEGREES-C ON THE MICROHARDNESS OF MGAL2O4 SPINEL, Journal of nuclear materials, 215, 1994, pp. 1096-1100
High-purity specimens of stoichiometric MgAl2O4 single crystal spinel
and a hot-pressed polycrystalline ceramic spinel were irradiated to ex
posures as large as 24.9 x 10(22) n Cm-2 (E > 0.1 MeV) in FFTF at 385
and 750 degrees C. The specimens did not develop any brittleness or fr
agility, and maintained their physical integrity. Microhardness measur
ements revealed that initially all specimens hardened a small amount a
nd then recovered slightly. At the lower irradiation temperature, the
dependence of microhardness on orientation observed prior to irradiati
on tended to disappear. There was also some evidence that a secondary
slip system was being activated. Following 750 degrees C irradiation,
the orientation dependence was not lost, and the evidence for activati
on of a secondary slip system was stronger.