C/C composites are the most promising candidates as high heat flux com
ponent materials, where temperature dependence of mechanical propertie
s and gas desorption behavior at elevated temperature are important pr
operties. At the beginning, the newly developed internal friction meas
urement apparatus, which enables the accurate measurement of dynamic e
lastic properties up to 1373 K along with the measurement of gas desor
ption behavior, was used. The materials studied were unidirectional (U
D) C/C composites reinforced with mesophase pitch-based carbon fibers,
which were heat treated at temperatures ranging from 1473 to 2773 K w
hich produced a variety of graphitized microstructures. Two-dimensiona
l (2D) C/C composites reinforced with flat woven fabrics of PAN type c
arbon fibers were also studied. These materials were heat treated at 1
873 K. From the temperature spectrum of internal friction of 2D C/C co
mposites, three internal friction peaks were detected and were related
to gas desorption. Also the temperature dependence of Young's modulus
of UD C/C composites, negative and positive dependence of Young's mod
ulus were observed reflecting microstructure changes resulting from th
e heat treatments.