D. Singh et al., EFFECT OF PROCESSING VARIABLES ON INTERFACIAL PROPERTIES OF AN SIC-FIBER-REINFORCED REACTION-BONDED SI3N4 MATRIX COMPOSITE, Journal of the American Ceramic Society, 77(10), 1994, pp. 2561-2568
Fiber/matrix interfacial debonding and frictional sliding stresses wer
e evaluated by single-fiber pushout tests on unidirectional continuous
silicon-carbide-fiber-reinforced, reaction-bonded silicon nitride mat
rix composites. The debonding and maximum pushout loads required to ov
ercome interfacial friction were obtained from load-displacement plots
of pushout tests. Interfacial debonding and frictional sliding stress
es were evaluated for composites with various fiber contents and fiber
surface conditions (coated and uncoated), and after matrix densificat
ion by hot isostatic pressing (HIPing). For as-fabricated composites,
both debonding and frictional sliding stresses decreased with increasi
ng fiber content. The HIPed composites, however, exhibited higher inte
rfacial debonding and frictional sliding stresses than those of the as
-fabricated composites. These results were related to variations in ax
ial and transverse residual stresses on fibers in the composites. A sh
earlag model developed for a partially debonded composite, including f
ull residual stress field, was employed to analyze the nonlinear depen
dence of maximum pushout load on embedded fiber length for as-fabricat
ed and HIPed composites. Interfacial friction coefficients of 0.1-0.16
fitted the experimental data well. The extremely high debonding stres
s observed in uncoated fibers is believed to be due to strong chemical
bonding between fiber and matrix.