IMPROVED SYNTHESES OF SOME SUBSTITUTED 5,6-DIHYDRO-S-TRIAZOLO[3,4-B] [1,3,4]-THIADIAZOLES IN A MICROWAVE-OVEN

Authors
GUPTA R PAUL S GUPTA AK KACHROO PL
Citation
R. Gupta et al., IMPROVED SYNTHESES OF SOME SUBSTITUTED 5,6-DIHYDRO-S-TRIAZOLO[3,4-B] [1,3,4]-THIADIAZOLES IN A MICROWAVE-OVEN, Indian journal of chemistry. Sect. B: organic chemistry, including medical chemistry, 33(9), 1994, pp. 888-891
Citations number
12
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Indian journal of chemistry. Sect. B: organic chemistry, including medical chemistry → ACNP
ISSN journal
03764699
Volume
33
Issue
9
Year of publication
1994
Pages
888 - 891
Database
ISI
SICI code
0376-4699(1994)33:9<888:ISOSS5>2.0.ZU;2-L
Abstract
Considerable increase in the reaction rate has been observed with bett er yields in the syntheses of some substituted 5, 6-dihydro-s-triazolo [3, 4-b] [1, 3, 4] thiadiazoles by the condensation of 3-alkyl/aryl-4- amino-5-mercaptotriazoles (1) with various aromatic aldehydes (2) in t he presence of catalytic amount of p-toluenesulphonic acid in unsealed vessels by microwave irradiation using DMF as energy transfer medium.