Sa. Carss et al., HIGH-RESOLUTION F-19 NMR-SPECTRA OF SOLID FLUORINATED ORGANIC-COMPOUNDS, Journal of the Chemical Society, Chemical Communications, (20), 1994, pp. 2407-2408
It is demonstrated herein that a combination of high-power proton deco
upling and magic angle spinning can give acceptable high-resolution F-
19 NMR spectra of simple solid multi-fluorinated organic molecules, as
exemplified by three fluorosteroids.