EFFICIENT AND SAFE DEPROTECTION OF HINDERED SILYLATED ETHERS USING IN-SITU GENERATED HF

Authors
MABIC S LEPOITTEVIN JP
Citation
S. Mabic et Jp. Lepoittevin, EFFICIENT AND SAFE DEPROTECTION OF HINDERED SILYLATED ETHERS USING IN-SITU GENERATED HF, Synlett, (10), 1994, pp. 851-852
Citations number
11
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Synlett → ACNP
ISSN journal
09365214
Issue
10
Year of publication
1994
Pages
851 - 852
Database
ISI
SICI code
0936-5214(1994):10<851:EASDOH>2.0.ZU;2-K
Abstract
Hindered silylated ethers such as t-butyldiphenylsilyl or triphenylsil yl are readily cleaved at room temperature using in situ generated HF from the reaction of BF3.OEt2 with 4-methoxysalicylaldehyde.