Y. Yanase et al., ATOMIC-FORCE MICROSCOPY OBSERVATION OF SI(100) SURFACE AFTER HYDROGENANNEALING, Journal of the Electrochemical Society, 141(11), 1994, pp. 3259-3263
Hydrogen gas plays an important role in the epitaxial growth process,
acting as both a high temperature precleaning ambient and the carrier
gas during epitaxial growth. The effect of hydrogen on the morphology
and microroughness of Si(100) and Si(111) surfaces was investigated us
ing atomic force microscopy under an atmospheric air ambient. The Si(1
00) surface after H2 annealing showed a periodic terrace and step stru
cture reflecting the double-domain (2 x 1 + 1 x 2) reconstructed struc
ture. This structure was maintained even after subsequent HCl vapor et
ching and epitaxial layer deposition in the Si epitaxial process.