The progress of a multifactor simplex optimisation algorithm has been
plotted in a visual mode, after a reduction in the number of factors u
sing the statistic principal component analysis method. The effectiven
ess of the proposed graphic representation has been evaluated when app
lied to simplex previously published optimisation methods such as: col
orimetric determination of cholesterol, flow-injection spectrophotomet
ric determination of promethazine and synthesis of an industrial pyraz
olone. The procedure has also been applied to develop new experimental
analytical methods like the determination of arsenic trichloride by i
nductively coupled plasma atomic emission spectrometry.