SCANNING ELECTRODE QUARTZ-CRYSTAL ANALYSIS

Citation
N. Oyama et al., SCANNING ELECTRODE QUARTZ-CRYSTAL ANALYSIS, Analytical chemistry, 69(6), 1997, pp. 1023-1029
Citations number
20
Categorie Soggetti
Chemistry Analytical
Journal title
ISSN journal
00032700
Volume
69
Issue
6
Year of publication
1997
Pages
1023 - 1029
Database
ISI
SICI code
0003-2700(1997)69:6<1023:SEQA>2.0.ZU;2-O
Abstract
Principles and methods for scanning electrode quartz crystal analysis (SEQCA) as a technique for mapping distribution of mass and measuring interfacial rheology are described, In SEQCA, quartz crystal resonates in a region between a normal electrode and a microelectrode scanned o ver the opposite side of the normal electrode. The surface of the quar tz crystal plate just below the scanning electrode is monitored (overs canning mode), A prototype system for the scanning electrode quartz cr ystal analysis is constructed. The dependence of the resonance propert ies on the location of the scanning electrode is studied. As a result, it was found that the qualitative mapping of the mass distribution is possible in the lateral resolution of 1 (9 MHz quartz) to 2 (5 MHz) m m, Viscoelastic properties of the load on the quartz surface are also measured qualitatively.