Yl. An et al., HYDROTHERMAL SYNTHESIS AND CHARACTERIZATION OF A NEW POTASSIUM PHOSPHATOANTIMONATE, Journal of materials research, 9(11), 1994, pp. 2745-2746
A new potassium phosphatoantimonate with a composition of 4K(2)O.4Sb(2
)O(5). P2O5.8H(2)O, which crystallizes in a monoclinic system with a =
23.952 Angstrom, b = 9.515 Angstrom, c = 8.193 Angstrom, and beta = 1
24.77, was hydrothermally synthesized and characterized by powder x-ra
y diffraction, chemical composition analysis, x-ray photoelectron spec
troscopy, and P-31 MAS-NMR techniques. The potassium ion can be exchan
ged by other monovalent ions.