A high-resolution x-ray diffractometer and transmission electron micro
scope (TEM) are used to characterize the redistribution of As precipit
ates in Si delta-doped GaAs grown by molecular-beam epitaxy at low sub
strate temperature (230 degrees C). The analysis results indicate that
superlattice satellite peaks, as observed for samples annealed at 700
-900 degrees C for 10 min, are attributed to the formation of the GaAs
/As superlattice. Also; the intensity of satellite peaks in x-ray rock
ing curves and TEM observations reveals the varying degree of As preci
pitates confined on the Si delta-doped planes. Furthermore, the asymme
try of the satellite peaks clearly indicates the lattice expansion and
contraction of the annealed low-temperature epitaxial layers.