InxGa1-xAs/GaAs strained layer superlattices were studied by means of
double-crystal x-ray diffractometry (DCXD), transmission electron micr
oscopy (TEM), and selected area x-ray photoelectron spectroscopy (SAXP
S) depth profiling techniques. The quality of superlattices, strain in
the sublayers, and their thickness and chemical composition were eval
uated. The effect of the real superlattice structure on the shape of x
-ray rocking curves has been revealed. It was concluded that full iden
tification of nonperiodic defects and the initial stage of stress rela
xation can be determined by combining DCXD and TEM methods. The result
s of SAXPS depth profiling were found to be in good quantitative agree
ment with DCXD and TEM data. The linear dependence of depth resolution
Delta z on the sputtering depth, caused by sputtering induced develop
ment of heterointerface roughness was determined in SAXPS profiles.