We have reduced high-titanium lunar mare soil and iron-rich lunar volc
anic glass with hydrogen at temperatures of 900-1100 degrees C. Ilmeni
te is the most reactive phase in the soil, exhibiting rapid and comple
te reduction at all temperatures. Ferrous iron in the glass is extensi
vely reduced concurrent with partial crystallization. In both samples
pyroxene and olivine undergo partial reduction along with chemical and
mineralogical modifications. High-temperature reduction provides insi
ght into the optical and chemical effects of lunar soil maturation, an
d places constraints on models of that process. Mate soil and volcanic
glass ate attractive feedstocks for lunar oxygen production, with ach
ievable yields of 2-5 wt%.