Hc. Gu et al., ORIENTATION DEPENDENCE OF CYCLIC DEFORMATION IN HIGH-PURITY TITANIUM SINGLE-CRYSTALS, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 188(1-2), 1994, pp. 23-36
Cyclic deformation was studied in a series of high purity titanium sin
gle crystals with different orientations. The multiple step test metho
d was employed in low cycle fatigue with a closed-loop electro-hydraul
ic servo-controlled Instron machine and cyclic stress-strain curves we
re obtained. The surface morphology of the fatigued specimens was obse
rved with scanning electron microscopy, and dislocation structure was
analysed with transmission electron microscopy. The results show that
the cyclic responses and microstructures of titanium single crystals a
re sensitive to orientation. In the crystals oriented near the center
of the (0001) stereographic projection, single slip and/or cross slip
occur, planar dipole arrays and dislocation loops exist, and the cycli
c strain hardening rate is low; whereas for crystals, in which orienta
tions are favorable for double and multiple slip, cell structure is fo
und and the cyclic strain hardening rate is high. Cyclic twins with di
fferent morphologies and fine structures are observed in almost all sp
ecimens, and the higher the content of twins, the higher is the strain
hardening rate. Stacking faults are found in fatigued titanium especi
ally in the region of twins in spite of the high stacking fault energy
.