O. Lyckfeldt et al., PROGRESS IN THE FABRICATION OF SI3N4 TURB INE ROTORS BY PRESSURE SLIPCASTING, Journal of the European Ceramic Society, 14(5), 1994, pp. 383-395
The fabrication of silicon nitride components by pressure slip casting
has been studied. Simple as well as more complicated shapes such as s
pin test discs, with homogeneous microstructure, were produced using t
his technique. Prior to casting in a full-scale pressure casting machi
ne, fundamental studies of the casting behaviour of the slips were con
ducted using filter pressing experiments. Due to the coarse pore struc
ture of the polymeric mould material used special attention was given
to the slip proper ties in order to avoid slip penetration into the mo
uld and to obtain an adequate consolidation. Parameters like the degre
e of particle interaction and solid content as well as the pressure sc
hedule were investigated. Partially flocculated slips were found to gi
ve considerably faster castings and the obtained bodies sintered to ne
arly full density without deformations In pressure casting of spin tes
t discs with stabilized slips, optimization of the pressure schedule w
as required to avoid cracking caused by stress gradients.