THE TOMOGRAPHIC ATOM-PROBE - A 3-DIMENSIONAL NANOANALYTICAL TOOL ON ASUBNANOMETRIC SCALE

Citation
D. Blavette et al., THE TOMOGRAPHIC ATOM-PROBE - A 3-DIMENSIONAL NANOANALYTICAL TOOL ON ASUBNANOMETRIC SCALE, Journal of trace and microprobe techniques, 12(1-2), 1994, pp. 17-35
Citations number
11
Categorie Soggetti
Chemistry Analytical
ISSN journal
07334680
Volume
12
Issue
1-2
Year of publication
1994
Pages
17 - 35
Database
ISI
SICI code
0733-4680(1994)12:1-2<17:TTA-A3>2.0.ZU;2-Q
Abstract
The Tomographic Atom-Probe is a quantitative microanalytical instrumen t which provides three-dimensional maps of chemical heterogeneities in a metallic material on a subnanometric scale. The basic principle of this new generation of apparatus relies on field evaporation of materi al and the localisation of evaporated atoms on a position-sensitive mu ltidetector. Chemical Species are identified by time-of-flight mass sp ectrometry. 3D-reconstructed images of a nickel base alloy containing very fine particles (similar to 7 nm) are presented and illustrate the performance of the instrument.