THE USE OF THERMAL-ANALYSIS FOR THE STUDY OF THE CALCINATION PROCESS OF OXALATE PRECURSORS FOR THE SYNTHESIS OF HIGH-TC SUPERCONDUCTORS

Authors
VOS A MULLENS J CARLEER R YPERMAN J VANHEES J VANPOUCKE LC
Citation
A. Vos et al., THE USE OF THERMAL-ANALYSIS FOR THE STUDY OF THE CALCINATION PROCESS OF OXALATE PRECURSORS FOR THE SYNTHESIS OF HIGH-TC SUPERCONDUCTORS, Bulletin des Societes chimiques belges, 101(3), 1992, pp. 187-192
Citations number
20
Journal title
Bulletin des Societes chimiques belges → ACNP
ISSN journal
00379646
Volume
101
Issue
3
Year of publication
1992
Pages
187 - 192
Database
ISI
SICI code
0037-9646(1992)101:3<187:TUOTFT>2.0.ZU;2-#
Abstract
The decomposition of the oxalateprecursors Y2(C2O4)3.4BaC2O4 . (6 + n) CuC2O4 . xH2O for the synthesis of high T(c) superconductors and the i ndividual Y-, Ba-, Cu-oxalate components is investigated by DTA and by TGA coupled with FTIR.