FLOW-INJECTION SPECTROPHOTOMETRIC DETERMINATION OF HYRCANOSIDE IN TABLETS

Citation
P. Solich et al., FLOW-INJECTION SPECTROPHOTOMETRIC DETERMINATION OF HYRCANOSIDE IN TABLETS, Die Pharmazie, 48(3), 1993, pp. 194-196
Citations number
17
Journal title
ISSN journal
00317144
Volume
48
Issue
3
Year of publication
1993
Pages
194 - 196
Database
ISI
SICI code
0031-7144(1993)48:3<194:FSDOHI>2.0.ZU;2-Z
Abstract
A flow-injection spectrophotometric determination of hyrcanoside based on the well-known reaction with picric acid in alkaline media using s pectrophotometric detection at 486 nm is described. The calibration gr aph is rectilinear from 10-400 mg.l-1 hyrcanoside (r = 0.9997) with a relative standard deviation of 1.6% for the ten injections. The sampli ng rate was about 60.h-1 and the overall dispersion of the system was D = 5.7. This method was utilized for the content uniformity testing o f experimentally prepared tablets of hyrcanoside.