COMPLETE ANALYSIS OF THE H-1 AND C-13 NMR-SPECTRA OF 5-ISOPROPYLSULFONYL-2-NORBORNENES THROUGH THE APPLICATION OF 2-DIMENSIONAL NMR TECHNIQUES

Authors
MATTALIA JM SAMAT A FAURE R CHANON M
Citation
Jm. Mattalia et al., COMPLETE ANALYSIS OF THE H-1 AND C-13 NMR-SPECTRA OF 5-ISOPROPYLSULFONYL-2-NORBORNENES THROUGH THE APPLICATION OF 2-DIMENSIONAL NMR TECHNIQUES, Spectroscopy letters, 26(4), 1993, pp. 575-583
Citations number
9
Categorie Soggetti
Spectroscopy
Journal title
Spectroscopy letters → ACNP
ISSN journal
00387010
Volume
26
Issue
4
Year of publication
1993
Pages
575 - 583
Database
ISI
SICI code
0038-7010(1993)26:4<575:CAOTHA>2.0.ZU;2-H
Abstract
Total assignment of C-13 and H-1 NMR spectra of the 5-isopropylsulfony l-2-norbornenes 2 was achieved using the concerted application of two- dimensional homonuclear and heteronuclear chemical shift correlations. The stereochemistry of both the diastereoisomers endo 2a and exo 2b h ave been established using the magnitude of the proton coupling consta nts.