Ct. Bodur et al., EFFECTS OF HEAT-TREATMENTS ON THE MICROSTRUCTURE OF A YTTRIA ALUMINA-DOPED HOT-PRESSED SI3N4 CERAMIC, Journal of Materials Science, 28(8), 1993, pp. 2089-2096
The effects of post-sintering heat treatments on the microstructure in
an Y2O3-Al2O3-doped hot-pressed silicon nitride ceramic in an argon a
tmosphere were studied. The degree of crystallization of the secondary
crystalline phase depended more on the time than the temperature of t
he heat treatments. Analytical transmission electron microscopy studie
s revealed a spencite-(Y, N)-apatite solid solution as the secondary c
rystalline phase, while the aluminium content in the residual glass wa
s high.