Is. Golovin et al., THE STUDY OF MICROPLASTICITY MECHANISM IN TI-50WT.PERCENT-NB ALLOY WITH HIGH HYDROGEN CONTENT, Journal de physique. IV, 6(C8), 1996, pp. 289-292
The upper yield point (approximate to 700 MPa) appears at the compress
ion test curves (epsilon=0.024 sec(-1)) of b.c.c. Nb-50 wt.%Ti due to
the increase of hydrogen content from 0 to 0.2 wt.% and more and leads
to the non monotonous increase in compressive lower yield stress from
400 to 550 MPa. Taking into account close connection between macro- a
nd microplasticity of metallic materials the low frequency (similar to
2 Hz) amplitude dependent internal friction (ADIF) spectrum (gamma=1.
.60 . 10(-5)) in hydrogenized Nb-50 wt.% Ti and Nb samples are studied
. The ADIF investigation of the closed hysteresis loop ''loading-unloa
ding'' shows the dependence of its width from the hydrogen content whi
ch evidences the fact of dislocation unpinning from hydrogen atmospher
es in the 1/2 cycle of loading. The study of ADIF spectrum for samples
with different hydrogen content before and after torsion deformation
(gamma approximate to 2%) shows the sharp increase of IF level at gamm
a=1..10 . 10(-5) after approximate to 1 hour of natural ageing. At tha
t time the ADIF curves change its shape from Gamma-shape to U-shape. T
he amplitude range of the IF increase depends on the hydrogen content.
It is the interaction of hydrogen atoms with dislocations that caused
the above mentioned effect which has not been observed in hydrogen fr
ee samples. The time estimation For the formation of thermodynamically
stable hydrogen atmospheres on dislocations shows that hydrogen atmos
pheres could not follow the dislocation during compressive tests and t
hat leads to the upper yield point appearance.