It is well known that in thin metallic films, the anelastic and the el
astic properties show some characteristic features linked to the speci
fic microstructure. The studied films Cu30Mo70, with a typical thickne
ss of 200nm are deposited by Ion Beam Sputtering (IBS) on oxidised sil
icon (100) substrates. The measurements are performed on a vibrating r
eed device adapted for thin adherent films over a temperature range be
tween 20 degrees C and 450 degrees C. This paper reports the combined
results of internal friction, elastic modulus and internal stresses me
asured during thermal cycling. ''Direct'' observations of the microstr
ucture are performed by X-Ray diffraction. We have correlated the modi
fications of the mechanical properties with the structural evolution o
f these metastable systems.