Naval Research Laboratory (NRL) scientists have developed an instrumen
t that has extreme sensitivity to energy dissipation in mechanical res
onators. While previous instruments measured loss to one part in ten,
the new instrument measures mechanical loss to one part in 10(4) or be
tter. Low defect levels, that result in small residuals of loss above
background, are detectable because of the instrument's high resolution
. We have used the resonator to examine loss spectroscopy of quartz re
sonators vibrating in flexure. The resonators have a large background
loss that peaks up at low temperature. Although the peak very closely
fits a Debye-like equation, the derived parameters, such as the decay
time prefactor, are unphysical.