Cb. Scruby et Hng. Wadley, TEMPERING EFFECTS ON ACOUSTIC-EMISSION MICROSTRUCTURAL RELATIONSHIPS IN FERRITIC STEELS, Journal of Materials Science, 28(9), 1993, pp. 2501-2516
A systematic study of the effect of tempering on acoustic emission-mic
rostructure relations has revealed that intermediate tempering treatme
nts of three Fe-3.25 wt % Ni alloys with 0.06, 0.17 and 0.49% carbon l
ead to a pronounced acoustic activity during subsequent ambient-temper
ature tensile testing. The maximum emission intensity occurs from samp
les tempered near 250-degrees-C for 100 min, and increases with carbon
content. Mechanical property measurements reveal the emission maximum
to be correlated with strengthening, the maximum strengthening (betwe
en 250 and 300-degrees-C) coinciding with the maximum emission. The ob
servations can be accounted for by a model which involves the high-spe
ed cooperative motion of groups of dislocations over distances corresp
onding to the lath packet dimension. The mechanism that induces cooper
ative dislocation motion is suspected to be a precipitate shearing pro
cess, a process that has not been significantly considered for quenche
d and tempered ferritic steels before. A second, much weaker source of
emission has been identified in material subjected to prolonged tempe
ring at 625-degrees-C. The mechanism responsible for this emission is
believed to be the rapid multiplication, and high-speed propagation, o
f groups of dislocations between widely distributed cementite particle
s. No evidence has been found to support the view that carbide fractur
e in quenched and tempered steels is a direct source of acoustic emiss
ion.