A. Krell et P. Blank, TIC-STRENGTHENED AL2O3 BY POWDER TAILORING AND DOPING PROCEDURES, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 161(2), 1993, pp. 295-301
High-carbide Al2O3/TiC composites have been fabricated without hot-pre
ssing by different processing techniques. Transient liquid phase sinte
ring with additions of TiH2 turned out to be the most promising of the
doping procedures. The highest strength, (> 800 MPa), however, was me
asured when omitting all additives and using a tailored alumina raw ma
terial with narrow grain size distribution. The influence of the alumi
na grain size distribution on sintering and strength is discussed as b
eing associated with the amount of grains and aggregates larger than 1
mum and with the mutual homogenization of oxide and carbide component
s. In contrast, the reduction of the median powder grain size plays a
minor role only.