We have grown a series of CeO2-YBaCu3O7 superlattices by pulsed laser
deposition. The purpose was to study the growth of an insulator - high
temperature superconductor system on a subnanometre scale. This is im
portant for superconducting devices, since the superconducting coheren
ce length is of the order of one to a few nanometres. The scale of the
superlattices ranges from a period of about 10 nm down to about 3 nm.
The structure of the layers was studied using X-ray diffraction and t
ransmission electron microscopy. We found that superlattices have a co
herent, epitaxial structure. The CeO2 follows the Frank - van Merwe gr
owth mode, where the growth proceeds by growing islands about 2 nm thi
ck that coalesce to form a continuous CeO2 layer at an average thickne
ss of 2 nm. We see no evidence of chemical mixing between the YBa2Cu3O
7 and CeO2, which implies that they are mutually insoluble at the grow
th temperature. We have characterized the superconducting properties o
f the layers using a microwave cavity method at 30 GHz. If the CeO2 la
yers are thin enough, the superlattices have similar surface resistanc
e and critical temperature as pure YBa2Cu3O7 filMS.