CRYSTAL AND MOLECULAR-STRUCTURE OF THE (-)-N-HYDROXYIMIDE OF (10-PINENE-2-YL) SUCCINIMIC ACID

Authors
KAROLAKWOJCIECHOWSKA J KWIATKOWSKI W MARKOWICZ SW
Citation
J. Karolakwojciechowska et al., CRYSTAL AND MOLECULAR-STRUCTURE OF THE (-)-N-HYDROXYIMIDE OF (10-PINENE-2-YL) SUCCINIMIC ACID, Journal of crystallographic and spectroscopic research, 23(5), 1993, pp. 423-429
Citations number
12
Categorie Soggetti
Crystallography,Spectroscopy
Journal title
Journal of crystallographic and spectroscopic research → ACNP
ISSN journal
02778068
Volume
23
Issue
5
Year of publication
1993
Pages
423 - 429
Database
ISI
SICI code
0277-8068(1993)23:5<423:CAMOT(>2.0.ZU;2-5
Abstract
Two independent molecules in the unit cell are the same enantiomer of the title compound but possess slightly different conformations. Both conformers are joined by H-bonds to one water molecule. The configurat ion at C11 was established as R. Crystal data: C14H19O3N x 1/2H2O; tri gonal, P3(2); a = 17.486(2), b = 17.486(2), c = 8.024(1) angstrom; V = 2124.72(6) angstrom3; Z = 6; lambda(CuKalpha) = 1.54178 angstrom; F(0 00) = 834; final R = 0.0495 for 2376 reflections (of 2747 unique data) .