THE SYNTHESIS OF NOVEL POLYCYCLIC HETEROCYCLIC RING-SYSTEMS VIA PHOTOCYCLIZATION .10. SYNTHESIS AND STRUCTURE DETERMINATION OF NAPHTHO[1',2'-4,5]THIENO[3,2-A]-4,7-PHENANTHROLINE
Mj. Musmar et al., THE SYNTHESIS OF NOVEL POLYCYCLIC HETEROCYCLIC RING-SYSTEMS VIA PHOTOCYCLIZATION .10. SYNTHESIS AND STRUCTURE DETERMINATION OF NAPHTHO[1',2'-4,5]THIENO[3,2-A]-4,7-PHENANTHROLINE, Journal of heterocyclic chemistry, 30(2), 1993, pp. 487-492
aphtho[1',2':4,5]thieno[3,2-a]-4,7-phenanthroline, a novel hexacyclic
ring system has been synthesized in four steps. The H-1 and C-13 nmr a
ssignments have been made using two-dimensional nmr techniques. The te
rtiary helical structure was determined by X-ray crystallographic anal
ysis.