Pk. Sinha et al., IN-VITRO EVALUATION OF MATRIX-BOUND FLUORIDE-RELEASING ORTHODONTIC BONDING ADHESIVES, American journal of orthodontics and dentofacial orthopedics, 111(3), 1997, pp. 276-282
Sustained fluoride-releasing composite resins have the potential to pr
event decalcification of enamel that may occur during the course of or
thodontic treatment. The purpose of this study was to evaluate the pot
ential of matrix-bound fluoride-releasing adhesives (MBF) for orthodon
tic use by comparing the shear bond strengths (in MPa) and remnant adh
esive on debonding (ARI scores) of these resins with commercially avai
lable orthodontic adhesives. Two types of resins were evaluated in sep
arate groups: The light-cured resins (group I) consisted of two light-
cured MBF, designated resins LA and LB, and five nonfluoride releasing
resins, designated LC, LD, LE, LF, and LG. The self-cured resins (gro
up II) consisted of one MBF, designated resin SA, and six nonfluoride
releasing resins, designated resins SE, SC, SD, SE, SF, and SG. These
resins were used to attach upper right central incisor metal (foil mes
h based) orthodontic brackets to 210 freshly extracted bovine incisors
in groups of 15 each. Student-Newman-Keuls multiple comparison tests
were performed at p < 0.05 to determine significant differences among
the resin types. Resin LA was significantly higher in bond strength ((
x) over bar = 27.4 MPa) compared with LD and LG ((x) over bar = 18.9,
10.7 MPa, respectively). Further, LA demonstrated a higher mean bond s
trength compared with LB, LC, LE, and LF ((x) over bar = 21.9, 24.1, 2
4.3, and 20.8 MPa, respectively). Resin LB had significantly lower ARI
scores ((x) over bar = 0.33) compared with LF and LG ((x) over bar =
1.20 and 1.80). LA, LB, LC, LD, and LE ((x) over bar = 0.47, 0.33, 0.6
0, 0.73, and 0.73, respectively) were not significantly different in t
heir ARI scores. Resin SE demonstrated significantly lower bond streng
th ((x) over bar = 17.2 MPa) compared with SC, SD, SE, SF, and SG ((x)
over bar = 23.9, 23.7, 23.4, 23.8, and 22.9 MPa, respectively). Resin
SA ((x) over bar = 19.0 MPa) was not significantly different in bond
strength from SE, SC, SD, SE, SF, and SG. Resin SA demonstrated signif
icantly lower ARI scores (x = 0.73) compared with SD and SE ((x) over
bar = 2.13 and 1.87). Resin SA had lower mean ARI scores compared with
SE, SC, SF, and SG ((x) over bar = 1.00, 1.27, 1.13 and 0.87, respect
ively). Sustained fluoride-releasing (matrix-bound) orthodontic adhesi
ve systems demonstrated bond strength and ARI scores that compared fav
orably with commercially available orthodontic adhesives.