Since the pioneering work on the formation of amorphous alloys by Duwe
z and coworkers using rapid quenching, a number of different strategie
s for producing metallic glasses have emerged. However, the problem of
processing bulk amorphous alloys remains an elusive goal. We have bee
n exploring the possibilities of using a nanophase ultrafine amorphous
particles, of approximately 5 nm, that can be compacted into bulk for
ms in situ. We have used both joule heating and magnetron sputtering m
ethods to synthesize amorphous alloys of Ni-Ti, Ni-Tb, Pd-Y, and Ti-1A
l. These alloys were characterized by X-ray diffraction and differenti
al scanning calorimetry. Preliminary results on sintering, crystalliza
tion, and mechanical properties of these nanophase materials are discu
ssed.