M. Rievaj et al., MERCURY TRACES DETERMINATION BY VOLTAMMETRY ON GOLD FIBER MICROELECTRODE IN SOME FOOD SAMPLES, Chemicke zvesti, 47(1), 1993, pp. 31-33
Gold fibre microelectrode was applied for mercury traces determination
by differential pulse anodic stripping voltammetry in mushrooms. The
food sample decomposition procedure with concentrated HNO3 under eleva
ted pressure and temperature in a digestion device is described. The m
ethod was tested on synthetic samples spiked with Hg(ClO4)2. Sufficien
t decomposition of the organic matrix was reached during the sample pr
etreatment and no significant loss of mercury was observed.