COMPLETE H-1 AND C-13 NMR SPECTRAL ASSIGNMENT OF PENTACYCLO [6.4.0.0(2,6).0(5,9).0(4,12)]DODECANE DERIVATIVES AND STRUCTURE ELUCIDATION OF PENTACYCLO [6.4.0.0(2,6).0(3,11).0(5,9)]DODECANE
Fjc. Martins et al., COMPLETE H-1 AND C-13 NMR SPECTRAL ASSIGNMENT OF PENTACYCLO [6.4.0.0(2,6).0(5,9).0(4,12)]DODECANE DERIVATIVES AND STRUCTURE ELUCIDATION OF PENTACYCLO [6.4.0.0(2,6).0(3,11).0(5,9)]DODECANE, Magnetic resonance in chemistry, 31(6), 1993, pp. 578-584
Treatment of entacyclo[6,4.0.0(2.6).0(5.9).0(4,12)]dodecan-2-ol with c
oncentrated sulphuric acid produced the rearranged hydrocarbon pentacy
clo[6.4.0.0(2,6).0(3,11).0(5,9)]dodecane as the main product. High-fie
ld H-1 and C-13 NMR techniques were used in the structure elucidation
and assignment of the different NMR resonances of these two and relate
d compounds.