G. Friedbacher et M. Grasserbauer, ATOMIC-FORCE MICROSCOPY OF TECHNOLOGICAL AND BIOLOGICAL SAMPLES, Fresenius' journal of analytical chemistry, 346(1-3), 1993, pp. 58-60
Atomic Force Microscopy (AFM) has been successfully used to characteri
ze a variety of samples with different chemical composition. Polycryst
alline sample preparation techniques, cleaving and careful adjustment
of the imaging setup made it also possible to investigate materials wi
th non-ideal geometry (small size, rough sample surface) down to the a
tomic scale. Pressed CaCO3 powder samples of different origin have bee
n imaged with atomic resolution. Multilayer systems of AlGaAs/GaAs and
Si/GaAs on top of a GaAs substrate could be imaged readily. Single de
lta-layers of Si in GaAs could be resolved. The results demonstrate th
at simple sample preparation techniques and the implementation of chem
ical reactions can greatly enhance the analytical scope and applicabil
ity of AFM.