A NEW METHOD FOR IMMOBILIZATION OF CHIRASIL-VAL FOR GAS-CHROMATOGRAPHY

Authors
ABE I KOBARA H WASA T
Citation
I. Abe et al., A NEW METHOD FOR IMMOBILIZATION OF CHIRASIL-VAL FOR GAS-CHROMATOGRAPHY, Chromatographia, 35(9-12), 1993, pp. 503-505
Citations number
9
Categorie Soggetti
Chemistry Analytical
Journal title
Chromatographia → ACNP
ISSN journal
00095893
Volume
35
Issue
9-12
Year of publication
1993
Pages
503 - 505
Database
ISI
SICI code
0009-5893(1993)35:9-12<503:ANMFIO>2.0.ZU;2-7
Abstract
A method for the immobilization of Chirasil-Val has been studied based on the cross-linking which takes place between terminal silanols of C hirasil-Val and polyfunctional silanes. A leached, dehydrated and tetr amethoxysilane-treated glass capillary coated with silanol terminated Chirasil-Val containing 5 % tetraacetoxysilane as a cross-linking agen t showed a maximum extractability of 15 % without any loss of chiralit y.