Vf. Rudchenko et al., REACTION OF THE DIMETHOXYAMINYL RADICAL WITH TERTIARY NITROSOALKANES AS A METHOD FOR THE PREPARATION OF N-ALKYL-N'-METHOXYDIAZENE N-OXIDES, Bulletin of the Russian Academy of Sciences, Division of Chemical Sciences, 41(10), 1992, pp. 1922-1924
The reaction of the dimethoxyaminyl radical with functionally substitu
ted nitrosoalkanes (2) in a 2:1 ratio at 20-degrees-C gives the corres
ponding N-alkyl-N'-methoxydiazene N-oxides (3) as a single isomer in p
reparative yields.