Sh. Lee et al., ELIMINATION OF LARGE ARTIFICIAL PORES DURING THE HOT ISOSTATIC PRESSING OF PRESINTERED ALUMINA, Journal of the American Ceramic Society, 76(4), 1993, pp. 880-884
Shrinkage of large pores during hot isostatic pressing (HIP) of presin
tered alumina has been studied. When alumina specimens containing arti
ficially produced large spherical pores are HIP treated, pore shrinkag
e occurs predominantly by plastic deformation. When the temperature of
the HIP treatment is 1850-degrees-C, the pores appear to collapse wit
h particle fragmentation and sliding. The complete elimination of larg
e pores is hard to achieve, because the pressure of N2 gas entrapped i
n the pores increases with their shrinkage. The practical implication
of these results is that large voids or cracks inside ceramics can be
removed by using the proper pressure/temperature regime.