N. Ramachandran et al., R-CURVE BEHAVIOR AND FLAW INSENSITIVITY OF CE-TZP AL2O3 COMPOSITE/, Journal of the American Ceramic Society, 76(4), 1993, pp. 961-969
A ceria-partially-stabilized zirconia-alumina (Ce-TZP/Al2O3) composite
optimized for transformation toughening was used to demonstrate its f
law insensitivity due to R-curve behavior. Four-point bend specimens f
abricated with a controlled distribution of spherical pores showed nea
rly the same characteristic strength and strength variability (Weibull
modulus) as specimens fabricated without the artificial pores. In sit
u observations confirmed stable growth of cracks initiated at pores an
d the crack lengths at fracture instability were much greater than the
pore sizes, thus resulting in fracture strengths insensitive to the p
ores. The small variability in the fracture strength was found to be a
ssociated with variability in the R-curve and the instability crack le
ngths. An analysis based on the fracture instability criterion for ris
ing crack growth resistance accounted for the strength variability due
to variability in the R-curve. Comparable four-point bend experiments
were also conducted on a sintered yttria-partially-stabilized zirconi
a (2Y-TZP) ceramic. This ceramic showed significant degradation of str
ength due to the presence of the pores. This flaw sensitivity is attri
buted to its steep rising R-curve over short crack lengths.