Hr. Kokabi et al., A NEW DEVICE FOR ELECTRICAL-RESISTIVITY MEASUREMENTS AS A FUNCTION OFTEMPERATURE (86-K 700-K) UNDER CONTROLLED-ATMOSPHERE BY THE 4-PROBE METHOD, Review of scientific instruments, 64(6), 1993, pp. 1549-1553
A device for measuring electrical resistivity as a function of tempera
ture using unsoldered, sharp, and independent contacts has been develo
ped. The probes are fixed on fine ceramic tubes, which are actuated by
pressure-sensitive springs. The ceramic tubes are guided by metallic
struts that also serve as thermal screens. The device is placed in an
enclosure where a primary vacuum is established and introduce a neutra
l, reducing, or oxidizing gas. Measurement can be performed continuall
y between 86 and 700 K. Materials having resistivities in the 10(-8)-1
0(6) OMEGA m range have been characterized even when they present resi
stivity jumps of many orders of magnitude.