Visible absorption spectroscopy and Small Angle Neutron Scattering (SA
NS) have been performed on soluble copolymer polystyrene-polyacetylene
(PS-PA). Two main results are discussed in detail. One concerns the m
icelle like structure of the copolymer in solution, the second the rev
ersible phase separation observed as a function of temperature. This l
atter result is promising, it should allows to prepare thin films with
controlled structure.