IMMOBILIZATION OF REAGENTS BY POLYMERIC MATERIALS - DETERMINATION OF METAMIZOL

Citation
Ll. Zamora et Jm. Calatayud, IMMOBILIZATION OF REAGENTS BY POLYMERIC MATERIALS - DETERMINATION OF METAMIZOL, Talanta, 40(7), 1993, pp. 1067-1071
Citations number
9
Journal title
Talanta
ISSN journal
00399140 → ACNP
Volume
40
Issue
7
Year of publication
1993
Pages
1067 - 1071
Database
ISI
SICI code
0039-9140(1993)40:7<1067:IORBPM>2.0.ZU;2-Q
Abstract
A method for immobilization of inorganic reagents, based on the disper sion of the reagent into an unsaturated polyester solution is applied to immobilization of lead dioxide. The obtained solid is of applicatio n in a flow-injection manifold for indirect atomic absorption determin ation of metamizol in pharmaceutical formulations. The procedure gives a linear calibration graph up to 6 ppm of metamizol with a relative s tandard deviation of 1.6% (3.0 mg/l) and a sample throughput of 72 hr- 1.