A method for immobilization of inorganic reagents, based on the disper
sion of the reagent into an unsaturated polyester solution is applied
to immobilization of lead dioxide. The obtained solid is of applicatio
n in a flow-injection manifold for indirect atomic absorption determin
ation of metamizol in pharmaceutical formulations. The procedure gives
a linear calibration graph up to 6 ppm of metamizol with a relative s
tandard deviation of 1.6% (3.0 mg/l) and a sample throughput of 72 hr-
1.